Beilstein J. Nanotechnol.2013,4, 94–102, doi:10.3762/bjnano.4.11
Abstract Four novel organotin(IV) complexes containing phosphorictriamide ligands were synthesized and characterized by multinuclear (1H, 31P, 13C) NMR, infrared, ultraviolet and fluorescence spectroscopy as well as elemental analysis. The 1H NMR spectra of complexes 1–4 proved that the Sn atoms adopt
complexation.
Keywords: luminescence; nanoparticles; organotin(IV) complexes; phosphorictriamide; ultrasonic; Introduction
In recent years, the increasing progress in the preparation of nanomaterials has led to characterization of a great number of nanostructures [1]. Nanoscale materials are of significance
, there are no reports about the preparation of nanosized organotin(IV) complexes bearing phosphorictriamide ligands.
In this work, following on from our previous works to prepare organometallic compounds including phosphorictriamide ligands [17][18], novel organotin(IV) complexes with the formula SnCl2
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Scheme 1:
The preparation pathway of organotin(IV) complexes 1–4.